making things happen with electron microscopes🔬 she/her 🐘: chaos.social/@isabel 🦋: bsky.app/profile/beamshift.b…

back focal plane (oregon)
ohh mein Gott die Röntgensicherheitsschraubendreher
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PSA
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rare x-ray safety screwdriver
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digital scan control on a JEOL 840 with the OBI (open beam interface). you can build it yourself for ~$600 in parts. old SEMs still get great resolution! you could turn this into an ebeam lithography setup too
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> buy de-ionized water > there’s H3O+ and OH- in it
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did a double take when I realized this was not vacuum grease but HAND CREAM?
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Someone should really pick up this RCA EMU (1940s TEM) on eBay and put it in a museum ebay.com/itm/196012616442
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FEI engineer: We need icons for the electron and ion gun diagnostics Graphic designer: I got this
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Vector and raster based position control, fully stream-based: there is no frame buffer, you can read and write an arbitrary number of points with low latency. lots of automation potential!
Introducing the first open source SEM digital image capture solution, the Open Beam Interface! GitHub: github.com/nanographs/Open-B… Bring your analog SEM into the digital world, all over one USB type-C connection. Taking orders now for our first batch of 6 boards, DM for details.
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this is an analog storage oscilloscope! I’m moving the beam in x and y with the knobs, and the signal persists on the display. there’s no digital memory, it’s just a special CRT.
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it was a nice thought though
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but actually, it opens the Danger Window into the electron gun of this SEM
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forbidden high-voltage peanut butter
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it’s SEM Startup Saturday
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Mr Clean Magic Eraser low mag
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be not afraid
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how do you quantify the value of preventative maintenance?
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Replying to @quantumbeans
southwest airlines and FEI stay winning
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o chem student (me) reacts to semiconductors
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here’s a shot from our teardown demo! this is an ice40 FPGA that @nanographs milled a trench through with a FIB, and then we put it in an SEM to get clearer images of the cross section. This is at about 20kx
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accidentally combined the 0.1% resistors with the identical 1% resistors
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1955 tube flip-flop
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step 1 of retrofitting a scan controller onto a SEM: find the x and y signals
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our live scan region-of-interest selection is pretty responsive
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Deflectors and stigmators
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Sample: Image:
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Just fired up this big plasma etcher (fits 8” wafers), going to see how it does cleaning microscope column & gun parts.
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Replying to @mycoliza
scratchy foam, this is what the microstructure looks like
Mr Clean Magic Eraser low mag
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simply having a wonderful Christmas TEM
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Just one of those days
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This dewar has style
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I’m a big fan of CM series control consoles, all the right knobs in all the right places
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Zeiss teardown today
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iCE40 my beloved
This Valentines day - what chip did you first fall in love with?
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deionized water, I put that shit on everything
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big prints of SEM images (24” x 32”) make great lab decorations!
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clicky buttons >>>>
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Detector says 😲
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Op amp data sheets:
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I made a tik tok
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another day another FIB cross sectioning live stream, this time the theme is MEMS
Tonight we are going to use the beam of gallium ions to cut open some MEMS microphones from @adafruit. After that we have some other MEMS devices we could put under the scope, join in the chat to help us decide. Starting at 5:30 PST piped.video/live/efyNGsUglvc?
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I love him
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more specialty tools that ship with electron microscopes: Extra Short Screwdriver and Extra Long Screwdriver
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emergency scope maintenance trip today - why is it always a hair?
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path artifacts everywhere
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old video of convergent beam diffraction; real space to reciprocal space and back ✨ every diffraction spot contains a dark field image!
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We want to hear about your cursed problem child “it should work but it doesn’t” microscope. Will fly to see your mystery background noise, intermittently wobbly goniometer, melted down lens bay, Win10 migration nightmare, etc. and find creative and affordable solutions
Hey if any of y'all need help with your Electron Microscope, we have availability in our field support schedule.
 We work on SEM TEM and FIB, and do a lot more than just service - including applications and methods development, custom tooling for service and sample prep, (1/2)
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Tomorrow’s all-day demo will be “how to speed run installing two electron microscopes and an ion beam”. It will be extremely hands on :) #teardown2023
@nanographs announcement: we are building a temporary electron microscopy lab in an art classroom for #Teardown2023! bring samples and let’s look at tiny things! plus we will be demoing a pretty cool new project.
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Working on ion beam things with @nanographs
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pushed more notes to @nanographs "digital notebook" datacore.nanographs.io, topics include: - thermograms - forklifts - TEM alignment - surfactants @obsdmd is the glue that holds it all together
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a PC that also has an SEM inside
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Chiller maintenance day
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FIB 200 is here
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Time for the “lubricate and install a high voltage bushing without making any dick jokes” challenge
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"Just add water" pancake mix under SEM. Looks like blobs of buttermilk/oil and crystals of baking soda in a sticky gluten substrate
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Leak reveal: This flange developed some pinholes in the weld around the IR camera port We put some good ol JB weld on it, pressure dropped by an order of magnitude
vacuum leak sleuthing setup (you’ll never guess where this chamber was leaking from)
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For everyone who asked how we were going to get the scopes out of the building:
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the Ansel Adams of the microcosmos
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pneumatic crimping tool set up ✅ anyone need any D-subs?
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DB235 chamber getting some fresh air
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CFEG bakeout is coming along nicely. Almost time to attempt tip startup 🤞
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Sometimes I miss being a commercial TEM analyst but my camera roll reminds me what it actually looked like:
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breaking news: electrons BLUE?
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Replying to @quantumbeans
green confirmed
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For a quick check, hold a flat piece of aluminum foil in an ultrasonic cleaner for a minute and you can see where and how much cavitation is happening
I wanted to see where the hotspots in my ultrasonic cleaner are and which water levels to avoid to get the most even pressure distribution 😄
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Based on my experience servicing electron microscopes & working in labs - well maintained equipment is highly correlated with the ability of an organization to make decisions effectively
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broad question for CNC machine owners, re: Clunkers - how feasible/economical/practical is retrofitting modern electronics onto machines that use hard drives and punch cards vs. getting a whole new machine? what capabilities do new machines have that old ones don’t?
A Bootstrapper's Guide to Re-Industrializing America I’m a big fan of focusing on things that are within my control. This article is about real actions we can take while we’re waiting for lawmakers to get their shit together. @andrewmccalip, @zanehengsperger, and others have been writing great articles about reindustrializing, and I wanted to say HELL YES to everything I’ve read so far. I fully believe that their policy ideas need to be implemented in parallel, but I’m not one to wait around for lawmakers to make my life better. This article isn’t about starting new billion-dollar foundries, refineries, or nuclear power…that is way over my head. I’m talking about what a couple of guys can do, in their own town, and support a family (and a healthy number of employees and their families). Rely on yourself. Just go do stuff. The CNC manufacturing boom in the 90s created thousands of entrepreneurs… **Example 1: CNC disrupts traditional talent** The 1990’s were an awesome time for US manufacturing. I was young, but I was able to experience the “modern” CNC wave first hand. My first hourly job was at a small sign shop in Minden, Nevada. The owner had built the business on his artistic talents: He could hand-paint about 20 different “alphabets” (fonts) by hand, from memory, on any surface from glass to the door of a pickup truck. Yes, it took a 6-pack to get the lines nice and straight, but damn he was good. Mac was a helluva artist, but he also knew that in order to keep up with demand, he needed to modernize. He invested some money in an early vinyl cutter/plotter so that younger staff (like myself) could make some of the simpler signs and graphics. The Windows 3.1 CNC interface was primitive, but suddenly I could create an end product that didn’t require a lifetime of practice. The side effect of this technology was that it made a previously talent-dependent industry available to anyone with a PC and a checkbook. Sign shops popped up out of nowhere. Our tiny town had 3 or 4 within a couple years, and there were more entrepreneurs running vinyl plotters in their garage competing with us. Our owner’s 20 year head start evaporated within a few years. However, operational excellence, a good brand, and outstanding service protected him in the long run. The point I’m trying to make is that new technology created a wave of entrepreneurs that was overall net positive to the industry and consumers. A bunch of people left their corporate jobs to start their own businesses, and that’s something I think we can replicate today. Something similar happened in the world of fabrication and manufacturing: **Example 2: CAD/CAM makes manual equipment obsolete** In the late 90’s CAD/CAM systems were developed that actually worked and didn’t require manual operations, navigating punch card programmers, AS400 systems or even DOS. Suddenly fabricators saw that instead of hiring machinists with 20 years of experience, they could hire young guys who could navigate a Windows environment and spit out GCODE that actually worked on the new generation of machines. Again, a wave of entrepreneurial types took a chance on this new style of fabrication and spun up businesses left and right. I’ve heard some ridiculous-but-true stories of equipment salesmen selling equipment from the back of limos, shop owners wrecking new Porsches because they were too coked up, and many, many divorces caused by “new money.” Once again, the catalyst for all of this was new technology that enabled new entrants to get into the industry. Fabrication and manufacturing was no longer something that was guarded with the prerequisite of generational knowledge. …But then the CFOs/MBAs got ahold of things and threw it all away The US saw an explosion of growth in machine shops, fabricators, and manufacturers enabled by new tech. It created a lot of growth and wealth, and many of these companies scaled quickly. The only issue is that as they scaled, MBAs and CFOs started to get creative and look for even more margin. Offshore labor could add a few basis points of margin, so why not send some work overseas? Seems innocent, ya? The rest is history. (Before you comment, yes, I know that offshoring was happening before the 90s, but I was busy playing Duck Hunt so I’m not going to get into it) We can re-boom I think it’s time for a 90’s-style equipment-led re-boom. Machine shop owners that prospered in the 90s are retiring. They don’t want to invest in new equipment to be competitive, they are tired. They’ve been doing this shit for 30+ years…it’s time for someone else to take their place. I don’t see machine shop retirement or closing as a bad thing. I think it opens up some room for new entrants, using new technology. The current generation of manufacturing equipment is light years ahead of anything from 1995…or even 2015. (Caution, wild generalizations ahead, bear with me) The Human/Machine Interfaces are easy to use, CAD/CAM software is the best it’s ever been, equipment uptime is up and maintenance needs are down. There has never been a better time to invest in new equipment and go win some work. I believe that if more brave entrepreneurs leverage this new technology and take the plunge into manufacturing, thousands more will follow. The reason manufacturing is hard is because many of the existing companies are saddled with old tech that is hard to learn, maintain, support and expand. A fresh start is what we need. “But Jim, all that new equipment is expensive! How do I buy it?” Use Other People’s Money - Specifically, The equipment manufacturer’s money There’s a lot of talk about how the government should offer low-interest loans to manufacturers for reindustrialization, and I agree wholeheartedly. But who knows how long that might take. I did an SBA loan years ago and just the application process took 6 months. Who knows how long it’ll take for new legislation to make its way down to the guy trying to get the loan. Something you can do now is choose a manufacturer that offers in-house financing (or has a finance subsidiary), like Haas, Amada America, or dozens of others. We’ve been able secure very attractive terms from in-house lenders, mostly because they exist to sell more equipment, they aren’t a bank. I’ve seen 0% down, 0% interest, delayed 1st payments, cash back…everything is on the table if you ask. Especially if that ask is at the end of the Sales guy’s quarter. Manufacturer financing can be such a massive advantage for a startup, and it doesn't dilute your equity like a VC would (VCs shouldn’t be in manufacturing, too much pressure to grow too fast). You’ll need all the advantages you can get to compete against China. “But Jim, how can a small manufacturer like me compete against China?” Do what China does, but better China will continue to be the lowest cost provider for commodity goods until we can outpace them with scale. That will take a while. Their cost of living is cheap, labor is cheap, their raw materials are cheap (subsidized?), and somehow they can ship something from China to Wisconsin for less than I can ship something to the next state…wtf (we need to eliminate the Terminal Dues System, but that’s another topic). So, I suggest we don’t compete with them on mass-produced commodities, yet. That will take loads of scale that is beyond the scope of this article. Instead, we can all pull a few pages from their playbook and use them to win work here in the US. **Follow up.** China is pretty damn good at being responsive. If you send a quote over, any time of day or night, you’ll usually have a response within an hour, usually minutes. Go try aliexpress if you don’t believe me, you’ll get about 30 emails per hour until you buy. And once you pull the trigger, they will be cutting chips before some guy in Ohio answers the first email. American manufacturers have to focus on being responsive and having the best communication in the world. I don’t care how you do it, just respond. Recently, I wanted to get a quote on a yard cleanup at my house to prep everything for winter. I called/emailed six companies that I found on Google. Four never responded. One scheduled a time nine days later to come give me a quote and didn’t show. One looked on Google maps to see how big my yard is, called to ask a few questions about the property, and gave me a quote during the same call. They won the job. The work is out there if you call people back. **Your customers work 24/7, so should you.** Respond via text, email or DM as many hours of the day as you can. If you need to sleep, hire someone, use an answering service or virtual assistant service. They pay for themselves on the first job. Modern customers don’t work 9-5, Monday-Friday. We get orders around the clock, 7 days a week, and I know the demand is there for other manufacturers too. Personally, I do the majority of my shopping for new equipment on the weekends when I have some time to think and browse websites. It’s unfortunate that I typically don’t hear back from anyone until Tuesday or Wednesday, usually later (if at all). **Put your price on the website!** CNC guys: Lean into instant quoting software, it’s out there and it’s getting better all the time. We write our own pricing software, but there are some off the shelf options that will get you started. Product manufacturers: Yes, I know that there is a huge percentage of manufacturing that is custom and needs to be quoted, but if you can, put your prices on the website (Haas does a great job of this). If it’s fully custom, put a price range or a variety of examples. It’s a win for your customers because they can get their expectations and budgets aligned with what you offer, and it’s a win for you because you aren’t wasting time quoting products for people who can’t afford it. **Go faster damnit!** 8 week lead time ain’t gonna cut it. Run 3 shifts, run lights out, whatever you gotta do. The work is out there if you are fast, I promise. Today, if you are 8 weeks out, China will be 2 weeks or less (shipped). You gotta do it in 5 days. The nice thing about speed is that it insulates you from price. If China is going to take 2 weeks and it costs $1000, you can do it in 5 days and charge $2000 and still have loads of demand. 80% of the buying population is impatient, bad at planning ahead, or both (myself included). “Do you ever think about the fact that Dominos does customized built to order products with a lead time of 15 minutes, all through an instant pricing configurator based website? I do.” - @andrewmccalip **Document your process!** Make it repeatable. It’s sooo much easier to train this way. Training manuals, checklists, operations manuals, written policies. It’s a big investment of time at the beginning, but it’ll make your entire operation run smoothly for decades. You need a smooth operation so that you can be responding to customers and making things faster. **Compete on service.** Personally, I spend more to have good service (especially when I buy equipment), and there are many others out there like me. Sure, the product might be 15% more expensive, but if it comes with 200% better service, that’s the product I’m buying. As manufacturers, we need to be long term partners with our customers, and that means focusing more on service before and after the sale. This is an area where China can’t compete because once the sale is complete, they are moving onto the next target. American manufacturers need to take a few notes from the hospitality industry: Make it right for your customers when something goes wrong, overnight spare parts when they need them, beat deadlines, follow up a few weeks later and see how things are going. I’d love to see American manufacturing positioned as “we aren’t the cheapest, but we’re the best.” Yes, we need to find efficiencies to reduce our prices where possible, but we have competitive advantages in front of us in the form of speed, service, quality, support, and communication. The reason China is winning work is because they are cheap, decent quality, and pretty fast. If we can’t compete with cheap, we sure as hell can win on everything else. But I can’t get the material for what they are selling finished products for! I know, no one can get material for what they are getting it for. It’s pretty wild how cheap things are over there. But, that’s the reality so stop complaining and find a way to move forward. In addition to offering the best speed, service, quality, support, and communication, we can do a few things to be smarter about our operations. **Co-op buying systems (regional).** Manufacturing is incredibly fragmented in the US, and I think we can band together a bit better and streamline how we source raw materials. What would it look like to join together with 10 other machine shops in your city and purchase billet using a co-op entity? You’d have 10x the buying power, and potentially lower freight costs if you can order in larger quantities to a central location. And hopefully you can make a few friends in the industry and support each other. I know it works for us. Also, there are other raw material vendors besides McMaster. Don’t let their pricing dissuade you from entering the market. They are the best company on the planet for getting you what you need, delivered the next day, but when it comes to buying commodities, don’t rely on their pricing when running your margin forecasts. **Build your business where the raw material is.** This is what China is really good at. Want to start a sunglasses factory in China? You better do it in Wenzhou. There are over 2,000 eyeglasses companies in that region. You’d be starting with an entire supply chain ready to go, including the workforce. In the US, if you need lots of wood in your product, you might want to be in the Pacific Northwest. Need lithium because you’re making batteries? Go to Nevada. Steel? Try the Midwest. Need lots of power? Move near a dam or solar farm or nuclear plant. If you can’t compete because you decided to start an organic Aloe Vera lotion company in Michigan, I don’t feel bad for you. Try Arizona. **Make things that are heavy, complex, custom.** The more size, complexity, and customizability your product has, the more insulated you are against China. Don’t focus on making products that are tiny, simple and easy to duplicate. They will spin up a copycat factory and wipe you out. Instead, make big things that are challenging to ship halfway across the world. DHL’s maximum shipping weight for Economy Select is 154lbs. The fast version (Express International) is 66lbs. **Make things that are complex and need a lot of engineering.** Make things based on customer specifications, things that need collaboration between the customer and the manufacturer. That’s where US companies can’t be beat. Beyond bootstrapping - where I hope the government can help I know I said at the beginning that I wasn’t going to focus on long-term changes related to government policy, but there are a few things that I’d like to mention to help guide lobbyists and lawmakers: **Win over lawmakers with job creation.** Lawmakers love jobs. As manufacturers, we need to talk more about creating the next wave of high tech, high paying manufacturing jobs, and talk less about automating everything towards lights out. Yes, we’ll have robots and automation, but we’ll also have lots of great people around to engineer them, program them, and work side by side with them. The story has got to be about people, not robots. You are 100x more likely to get a grant or tax abatement by talking about job creation vs. a dark warehouse full of conveyors. **Build “Cash for Clunkers” v2.0 - but for equipment.** This is a big one for me, and I bet a few of you are connected enough to help me pull it off. Let’s do a government-backed cash for clunkers program, but for outdated manufacturing equipment. If you really want to reindustrialize the US, we gotta get rid of CNC machines still running on 5 ¼” floppy drives (or punch cards). I’d love to see some sort of credit towards a new machine if you “push pull or drag!” in your old machine, or show proof of recycling. Hell, we probably don’t even need the government to help here, a smart equipment manufacturer can just steal this idea and run with it. Amada, Haas, I’ll be first in line if you wanna test this out. **Government-backed loans to equipment manufacturers. ** Giving direct loans to startups is risky, and the government doesn’t have the bandwidth to vet all applications properly. Remember the PPP program during covid? That didn’t work out so good, except for the fraudsters who got Lambos. Instead, what if we gave equipment manufacturers (Haas, Fadal, Mazak, Amada, PEKO, Parker Hannifin) government-backed loans that they could use to offer better loan terms to the end user? Their sales teams are great at vetting customers, and they aren’t going to be as vulnerable to fraud as the government would. Every equipment sales person I know physically visits the operation, learns the business, gets to know the operator. The idea is to use the equipment manufacturers as a way to distribute the funds, in the form of cheap loans. Conclusion If you sell good equipment with good terms and flexible financing, people will build a business around that equipment. I have seen it happen in 1995 (Modern CNC equipment), 2005 (iPhone Apps), 2015 (CNC plasma tables) and now in 2025 (next-gen manufacturing equipment). Haas helped create more manufacturing entrepreneurs in the last 20 years than any other company I can think of, and I believe we can scale that model 100x. If we can show young entrepreneurs that manufacturing is actually really fun (Factorio in real life), and it doesn’t require 20 years of experience (due to modern equipment and software) we’ll reindustrialize from the ground up, 2,500 square feet at a time.
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Saw this while eating Taco Bell, instant follow
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ICHIEMON??!!?!?!?
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Replying to @softminus
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120 kV FEG, 16 megapixel CMOS camera and hybrid pixel detectors… interesting
China unveiled its first domestically produced transmission electron microscope (TEM), the TH-F120, on Saturday, the Science and Technology Daily reported. The groundbreaking development marks a major breakthrough in core technologies and manufacturing capabilities of the country. globaltimes.cn/page/202401/1…
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just received these cute little tweaker screwdriver tools to ship with the Open Beam Interface boards, so you can tune the input/output ranges right out of the box.
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Microscopy slide rule collection
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video looks like it’s been compressed to shit, here’s the hair
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inspecting the PCB to see what the grounding situation is. reliable sources are telling me the designers of this board may have been using drugs at the time
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Replying to @tom_verbeure
but does your wife have 10 nm resolution?
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So hexagonal pixels are more efficient than square pixels because of the packing, are there image formats for hexagonal pixels?
Replying to @BreakingTaps
If we zoom in, we can see a honeycomb pattern! What?! I think we're seeing an artifact of my ebeam litho program 😅 I'm using a new, high resolution resist and I think it's showing the "pixels" of my raster scan. Each dwell corresponds to a white circle
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Hunting down a source of noise in our SEM images today, looking for ripple on the outputs of the power regulator. Pulling these water cooled assemblies out is a pain but there’s lots of test points in here
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the microscopy version of this: imagine if your Titan had schematics available like the CM200 did
Imagine if your MacBook had schematics available like the Commodore 64 did! #righttoreuse #righttorepair #retro #commodore
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I like when SEM footage pops up in sci fi movies Left: Blade Runner (1982) Right: Buckaroo Banzai (1984)
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Having fun here
Tomorrow’s all-day demo will be “how to speed run installing two electron microscopes and an ion beam”. It will be extremely hands on :) #teardown2023
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Vertical scan signal: brrrrrrrrrrrrr Horizontal scan signal: brbrbrbrbrbr
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FIBception
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it's an 840 for $375 in Maryland, here's the link if anyone wants to save a man from himself: gsaauctions.gov/auctions/pre…
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Just doing gremlin things
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@nanographs announcement: we are building a temporary electron microscopy lab in an art classroom for #Teardown2023! bring samples and let’s look at tiny things! plus we will be demoing a pretty cool new project.
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really low mag but still the world’s smallest nanographs logo
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vacuum leak sleuthing setup (you’ll never guess where this chamber was leaking from)
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Grandpa 35C is online and showing us diatoms
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excuse me high voltage tank, where is the beam I had on Friday?
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Zone axes
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went down a compustage rabbit hole recently, but it ended well and the stage is now error-free
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“Don’t talk to me or my son ever again”
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“what’s in my purse” sputter coater edition
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.@nanographs hard at work answering all of your questions about our open beam interface, meanwhile I made a cat hat
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Here’s an EMU in action and the kinds of images that came from it! Back in this era biologists were arguing over the existence of bacterial nuclei
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is there anything more beautiful than thousands of individually bagged connectors?
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made some little reference drawings for the back side
Open hardware, coming soon to a (electron or other) microscope near you.
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